Methyl Ethyl Ketone → Triethanolamine

HRID 2076732Notes

Reaction equation

HRID 2076732 reaction equation
COC(OC)([C:10]([C:12]1C=CC=CC=1)=[O:11])C1C=CC=CC=1.CC(C1C(O)=C(C(C)(C)C)C=C(CCC(OCCSCCOC(CCC2C=[C:54](C(C)(C)C)[C:53]([OH:60])=C(C(C)(C)C)C=2)=O)=O)C=1)(C)C.CC1(C)C(OC(CCCCCCCCC(OC2[C:91](C)(C)[CH2:90][NH:89]CC2(C)C)=O)=O)C(C)(C)CNC1.CCC(C)=[O:102]>C1(=O)CCCCC1>[N:89]([CH2:12][CH2:10][OH:11])([CH2:54][CH2:53][OH:60])[CH2:90][CH2:91][OH:102]

Participants

6

Reactant 4

HCID 6569Methyl Ethyl Ketone4×HCID 62018HCID 62018, compoundHCID 64883Thiodiethylene bis(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate)HCID 905712,2-Dimethoxy-2-phenylacetophenone

Product 1

HCID 7618Triethanolamine

Reagents, catalysts & solvents 1

HCID 7967CyclohexanoneSolvent

Procedure

A Part “B” solution was prepared by mixing 2.96 gm of 50% Ebcryl1290 in MEK, 1.29 gm of 28% Socal 322 (from Solvay Chemicals.) dispersion in cyclohexanone, 0.10 gm of 30% MEK-ST, 0.2 gm of a 25% poly-Q solution in MEK and 0.22 gm of a photoinitiator (PI) solution containing 24% of BMS, 12.7% of Irgacure 651, 2.4% of ITX, 6.34% of DBTDL and 1.58% of Irganox 1035 (thiodiethylene bis[3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate]) and 3.18% of Tinuvin 123 (decanedioic acid, bis(2,2,6,6-tetramethyl-1-(octyloxy)-4-piperidinyl)ester, reaction products with 1,1-dimethylethylhydroperoxide and octane from Ciba Specialty Chemicals) in MEK.

Workup

  1. customA Part “B” solution was prepared
  2. additionby mixing 2.96 gm of 50%

Sources & evidence

ORD record
ord-07e9209c57c448cf808225572be2045b
Source dataset
uspto-grants-2011_04
Patent number
US07927711B2

Reaction notes

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