Strontium carbonate → HCID 178526099, compound

HRID 2076755Notes

Reaction equation

HRID 2076755 reaction equation
[N+]([O-])([O-])=O.[Ag+:5].[C:6](=[O:9])([O-:8])[O-:7].[Sr+2:10]>[N+]([O-])([O-])=O.[Ag+]>[C:6](=[O:7])([O-:9])[O-:8].[Ag+2:5].[C:6](=[O:7])([O-:9])[O-:8].[Sr+2:10]

Participants

4

Reactant 2

HCID 15407Strontium carbonateHCID 24470Silver Nitrate

Product 1

HCID 178526099HCID 178526099, compoundYield 768.6%

Reagents, catalysts & solvents 1

HCID 24470Silver NitrateCatalyst

Procedure

100 g of an aqueous silver nitrate solution containing 10 g of silver nitrate was added dropwise to 245.0 g of a slurry solution containing 23.5 g of strontium carbonate having a surface area of 6.7 m2/g and an alkaline metal content of 20 ppm or less (manufactured by SAKAI CHEMICAL INDUSTRY CO., LTD., under the trade name of SW-K) as alkaline earth metal carbonate at 20° C. to 25° C., followed by stirring for 3 hours. The solid was collected by filtration, washed with 200 mL of ion exchanged water four times to obtain 193 g of a silver carbonate/strontium carbonate mixture. Then, a sliver catalyst was prepared by filling the resulting silver carbonate/strontium carbonate mixture in a calcinations glass tube, followed by subjecting to calcination at 350° C. for 3 hours under an air flow of 100 mL/min.

Workup

  1. customat 20° C. to 25° C.
  2. filtrationThe solid was collected by filtration
  3. washwashed with 200 mL of ion

Sources & evidence

ORD record
ord-f3b9f8dd706e49af9c5c4a4b59cc76bd
Source dataset
uspto-grants-2011_04
Patent number
US07928034B2

Reaction notes

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