HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59312356, compound → HCID 59312271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59312356 | HCID 59312356 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 59312271 | HCID 59312271 | 90% |
Reaction Steps
The title compound was prepared according to a similar method to that of Example 64, except that 10% palladium on carbon was used, starting from 2,7-dibenzyl-4-methyl-6,7,8,9-tetrahydro-5H-pyrimido[4,5-d]azepine of Preparation 39, and obtained as a pale yellow solid in 90% yield (44 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928099B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-8a95aa57741442aba788b27d3dc34c86 |
| Source note | uspto-grants-2011_04 |