Methylamine → HCID 59312251, compound

Participants

Reaction Steps

To a solution of the triflate from Step C (90.0 mg, 0.18 mmol) in DMA (2 mL) was added methylamine solution in THF (0.45 mL, 2.0M, 0.89 mmol) and the reaction was stirred for 48 h. The reaction mixture was concentrated in vacuo and the material was used without further purification. A quantitative yield was assumed. LRMS ES+ and AP+ m/z 387 [MH]+.

Provenance & Evidence