HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-(3-Chlorophenyl)-2-methylpropanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(3-Chlorophenyl)-2-methylpropanoic acid | HCID 15582644 | — |
| Product | 2-(3-Chlorophenyl)-2-methylpropanoyl chloride | HCID 13987531 | — |
Reaction Steps
2-(3-Chlorophenyl)-2-methylpropanoic acid (5.7 g, 28.7 mmol) was stirred in thionyl chloride (100 mL) for 2 hours at reflux. The thionyl chloride was removed under vacuum to give the product (5.69 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928139B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-e875b7ed7d81462790be6475de18cdd0 |
| Source note | uspto-grants-2011_04 |