HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178451294, compound → HCID 178429101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178451294 | HCID 178451294 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 178429101 | HCID 178429101 | — |
Reaction Steps
Tert-butyl 2-(2-hydroxy-1,1-dimethyl-7-(2-morpholinoethylamino)-4-oxo-1,4-dihydronaphthalene-3-carboxamido)acetate (25 mg, 53 μmol) was dissolved in TFA (2 mL) at room temperature for 30 minutes and concentrated to give crude product. The crude product was purified via preparatory TLC to give the title compound. MS (ESI) m/z: Calculated; 417.5: Observed; 418.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928139B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-fbf8f2c708fc4edaa686f0ae471307ca |
| Source note | uspto-grants-2011_04 |