反应详情

The triphenylsulfonium chloride aqueous solution of Synthesis Example 1 (0.0049 mole) and the sodium 4-benzoyloxy-1,1,2,2,-tetrafluorobutanesulfonate (0.0051 mole) synthesized above were stirred in 26 g of dichloromethane. The organic layer was separated and washed three times with 20 g of water. The organic layer was concentrated, obtaining 2.1 g of the target compound, triphenylsulfonium 4-benzoyloxy-1,1,2,2,-tetrafluorobutanesulfonate.

1. customThe organic layer was separated
2. washwashed three times with 20 g of water
3. concentrationThe organic layer was concentrated