HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylsulfonium chloride → Triphenylsulfonium 4-benzoyloxy-1,1,2,2-tetrafluorobutanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylsulfonium chloride | HCID 61343 | — |
| Reactant | Sodium 4-benzoyloxy-1,1,2,2-tetrafluorobutanesulfonate | HCID 86654883 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Triphenylsulfonium 4-benzoyloxy-1,1,2,2-tetrafluorobutanesulfonate | HCID 86654882 | — |
Reaction Steps
The triphenylsulfonium chloride aqueous solution of Synthesis Example 1 (0.0049 mole) and the sodium 4-benzoyloxy-1,1,2,2,-tetrafluorobutanesulfonate (0.0051 mole) synthesized above were stirred in 26 g of dichloromethane. The organic layer was separated and washed three times with 20 g of water. The organic layer was concentrated, obtaining 2.1 g of the target compound, triphenylsulfonium 4-benzoyloxy-1,1,2,2,-tetrafluorobutanesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07928262B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-cb2d2935d6274e4ab6aceef2c92b58b6 |
| Source note | uspto-grants-2011_04 |