Ethyl Spiro[2.5]octane-1-carboxylate → HCID 11820440, compound

Participants

Reaction Steps

The title compound was prepared as described in Example 1B substituting the product from Example 52B for the product from Example 1A. 1H NMR (DMSO-d6, 300 MHz) δ 1.34-1.43 (m, 3H), 1.11-1.19 (m, 4H), 0.95 (s, 3H), 0.93 (s, 3H), 0.92 (s, 3H), 0.87 (m, 1H), 0.85 (s, 3H), 0.82 (dd, J=4.0, 7.9 Hz, 1H); 13C NMR (DMSO-d6, 100 MHz) δ 19.3, 24.9, 25.7, 30.7, 30.9, 31.2, 31.5, 32.0, 32.4, 40.1, 48.7, 51.9, 173.2.

Provenance & Evidence