HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Cyclohexyl-3-(phenylmethoxy)benzeneethanamine → HCID 67103142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Cyclohexyl-3-(phenylmethoxy)benzeneethanamine | HCID 67103172 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67103142 | HCID 67103142 | — |
Reaction Steps
A stirred solution of the oil isolated in Step D (4.5 g, 14 mmol) and Pd/C (10%, 150 mg) in ethanol (100 mL) was hydrogenated under 1 atm of hydrogen overnight. The catalyst was filtered off, and the solvent was removed in vacuo to yield an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07932261B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-a4cb920704af493a87189b8772a3e32b |
| Source note | uspto-grants-2011_04 |