Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 2-Amino-4-bromobenzaldehyde | HCID 17914598 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178517417 | HCID 178517417 | 95% |
Reaction Steps
A mixture of 2-amino-4-bromobenzaldehyde (1 eq) and urea (14 eq) was heated to 180° C. in an oil bath under Argon for 1 h. Water was added to after cooling to ambient temperature. The solid was collected by filtration and air dried to give product in 95% yield. ES/MS m/z 225/227 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07932262B2 |
|---|
| Source dataset | uspto-grants-2011_04 |
|---|
| ORD ID | ord-1f41e7f7cd014e8f942972d3dde3615b |
|---|
| Source note | uspto-grants-2011_04 |
|---|
