反应详情

A mixture of 4-methoxy-3-nitrobenzotrifluoride and 10% of 10% Pd/C in methanol was stirred under H2 atmosphere overnight at room temperature. The reaction mixture was filtered through celite, concentrated and dried under vacuum to provide product as an off white solid in 99% yield. ES/MS m/z 192.1 (MH+).

1. filtrationThe reaction mixture was filtered through celite
2. concentrationconcentrated
3. customdried under vacuum
4. customto provide product as an off white solid in 99% yield