Hydrochloric Acid → HCID 66876317, compound

Participants

Reaction Steps

4M HCl in dioxane (15 ml) was added to ethyl 2-{3-[(tert-butoxycarbonyl)amino]azetidin-1-yl}pyrimidine-5-carboxylate (323 mg, 1 mmol) and the reaction stirred at r.t. for 30 min. The suspension was concentrated in vacuo to give the title compound as a white solid (323 mg, quant.). LCMS purity 78%, m/z 223 [M+H]+.

Provenance & Evidence