HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride hydrochloride → HCID 44192408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride hydrochloride | HCID 23392 | — |
| Reactant | 1-(tert-Butoxycarbonyl)-4-(methanesulfonyloxy)piperidine | HCID 4184869 | — |
| Reactant | HCID 57829224 | HCID 57829224 | — |
| Product | HCID 44192408 | HCID 44192408 | — |
Reaction Steps
Substituting 1-[2-(1H-indol-6-yl)-5-(2-trimethylsilanyl-ethoxymethyl)-5H-pyrrolo[2,3-b]pyrazin-7-yl]-2,2-dimethyl-propan-1-one for 1-[2-(1H-indol-5-yl)-5-(2-trimethylsilanyl-ethoxymethyl)-5H-pyrrolo[2,3-b]pyrazin-7-yl]-2,2-dimethyl-propan-1-one and 4-methanesulfonyloxy-piperidine-1-carboxylic acid tert-butyl ester for 2-chloromethylpyridine hydrochloride. MP=201-207 C., (M+H)+=402.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07932254B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-01d9d5bcad2a41e48d337ed784560fab |
| Source note | uspto-grants-2011_04 |