Hydrochloride methanol → HCID 23114814, compound

Participants

Reaction Steps

To t-butyl 3-[[5-chloro-4-[(4-chlorophenylsulfonyl)-(2,5-difluorophenyl)methyl]pyridin-2-yl]amino]propylcarbamate (70 mg, 0.13 mmol) was added a 20% hydrochloric acid-methanol solution (2 ml). The resulting mixture was stirred for 2 hours. The residue obtained by concentrating the reaction mixture under reduced pressure was crystallized from ethanol to give the title compound as a white solid (42 mg, 83%).

Provenance & Evidence