Methylamine → HCID 86646580, compound

Participants

Reaction Steps

A mixture of 0.25 gram (0.00083 mole) of 1-(2-{[(6-chloro(3-pyridyl))methyl](2-methylpropyl)-amino}ethylthio)ethan-1-one and 0.78 gram of a 33% solution of methylamine in ethanol (0.0083 mole of methylamine) in 50 mL of ethanol was stirred at ambient temperature two hours. The reaction mixture was concentrated under reduced pressure to a residue. This residue was use without further purification in Step E.

Provenance & Evidence