HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67101411, compound → HCID 67100937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67101411 | HCID 67101411 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67100937 | HCID 67100937 | — |
Reaction Steps
11.C.2 Hydrogenation of “E7” using 5% Pt/C as catalyst gives the compound 5-{5-[2-(pyridin-4-yl)ethyl]2,4-dimethoxyphenyl}-1-(2-chlorophenyl)-1H-pyrazole and ether cleavage thereof gives the compound 5-{5-[2-(pyridin-4-yl)ethyl]2,4-dihydroxyphenyl}-1-(2-chlorophenyl)-1H-pyrazole, retention time [min] 1.397, M+H+[m/e] 392.86.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07932401B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-f50e82fc5e7f456bbeed7eef274caadc |
| Source note | uspto-grants-2011_04 |