Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium t-butoxide | HCID 23676156 | — |
| Reactant | HCID 67103497 | HCID 67103497 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67103576 | HCID 67103576 | — |
Reaction Steps
The compound (303.8 mg) obtained in Example 14-2 and sodium t-butoxide (manufactured by Wako Pure Chemical Industries, Ltd.) (138.4 mg) were dissolved in anhydrous THF (6.0 ml) and the whole was stirred at 60° C. for 15 hours. After completion of the reaction, water was added thereto and the whole was subjected to extraction with chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07932281B2 |
|---|
| Source dataset | uspto-grants-2011_04 |
|---|
| ORD ID | ord-0134a6f5c53349bb88b84bf692e670dd |
|---|
| Source note | uspto-grants-2011_04 |
|---|
