Hydrochloric Acid → HCID 11671482, compound

Participants

Reaction Conditions

Reaction Steps

The compound (34.1 mg) obtained in Example 86-1 was dissolved in dioxane (1.0 ml) and added with concentrated hydrochloric acid (500 μl) at room temperature and the whole was stirred at an outside temperature of 100° C. for 4 hours. After completion of the reaction, the resultant was concentrated and evaporated to dryness under reduced pressure, thereby obtaining a hydrochloride (43.4 mg) of the subject compound as a white solid.

Provenance & Evidence