HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11664000, compound → HCID 11577273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11664000 | HCID 11664000 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 11577273 | HCID 11577273 | — |
Reaction Steps
The hydrochloride (200 mg) of the compound obtained in EXAMPLE 96-4 was dissolved in concentrated hydrochloric acid (3 ml) and water (0.2 ml), and the whole was refluxed under heating for 4 hours. After completion of the reaction, the solvent was distilled off, thereby obtaining a hydrochloride (175.1 mg) of the subject compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07932281B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-40fbcd08864943169b43d9a47847a98f |
| Source note | uspto-grants-2011_04 |