HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 19799188, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 19799190 | HCID 19799190 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 19799188 | HCID 19799188 | — |
Reaction Steps
The title compound is prepared from 2-(thien-2-ylmethoxy)ethyl hydroxylamine from Example 19 by first reaction with 3 equivalents of acetyl chloride and 3.3 equivalents of triethylamine followed by treatment with LiOH in 2-propanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183818 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-4a5da4b074b7477ea3ca3896b1c2f032 |
| Source note | uspto-grants-1993_02 |