HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 19799249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | 2,4-Piperidinedione | HCID 10887863 | — |
| Product | HCID 19799249 | HCID 19799249 | 94.2% |
Reaction Steps
A mixture of 4-fluoroaniline (978 mg) and 2,4-dioxopiperidine (1.0 g) was heated at 120° for 1 h, and then cooled. The solid was triturated with ether (30 ml) and the solvent was decanted to leave the title compound (1.71 g), m.p. 195°-198°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183820 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-b162d8ce95414641a0f59924eceafe9c |
| Source note | uspto-grants-1993_02 |