HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Toluidine → HCID 15712495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Toluidine | HCID 7242 | — |
| Reactant | 2,4-Piperidinedione | HCID 10887863 | — |
| Product | HCID 15712495 | HCID 15712495 | 97.8% |
Reaction Steps
A mixture of o-toluidine (943 mg) and 2,4-dioxopiperidine (1.0 g) was heated at 120° for 30 min. The oil was cooled, triturated with ether (30 ml) and the solvent was decanted to give the title compound (1.74 g), m.p. 155°-158°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183820 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-98d87b973b42465abb12b8a171a1ed2d |
| Source note | uspto-grants-1993_02 |