HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11819612, compound → HCID 10261633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11819612 | HCID 11819612 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 10261633 | HCID 10261633 | 89.5% |
Reaction Steps
7-Fluoro-1-methyl-1H-indole-2-methanol (2.0 g) was dissolved in 1,4-dioxan (50 ml). Manganese dioxide (2.91 g) was added and the mixture was heated at reflux for 1 h. The mixture was then filtered and the filtrate was evaporated in vacuo to give the title compound (1.77 g) as a solid, m.p. 61°-63°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183820 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-3541b782523b4765bc599f7ad6dbef4c |
| Source note | uspto-grants-1993_02 |