HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70047317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Lurosetron | HCID 172999 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70047317 | HCID 70047317 | — |
Reaction Steps
A solution of 6-fluoro-2,3,4,5-tetrahydro-5-methyl-2-[(5-methyl-1H-imidazol-4-yl) methyl]-1H-pyrido[4,3-b]indol-1-one (260 mg) in methanol (10 ml) was treated with ethereal hydrogen chloride and the mixture was then concentrated in vacuo. The residue was triturated with ether (15 ml) to give the title compound (230 mg) as a solid, m.p. 275°-278°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183820 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-2497383a90b54518a6ee12b6479af9a5 |
| Source note | uspto-grants-1993_02 |