HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodophenol → HCID 15070116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodophenol | HCID 10784 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Ethyl 5-bromovalerate | HCID 84580 | — |
| Product | HCID 15070116 | HCID 15070116 | 38.1% |
Reaction Steps
Under the conditions of example 2A, 3 g of 2-iodophenol in the presence of 8.9 g of cesium carbonate is reacted with 2.84 g of 5-bromovaleric acid ethyl ester, worked up, and 1.8 g of 5-(2-iodophenoxy)valeric acid ethyl ester with a boiling point of 210° C./0.4 mbar is obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183925 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-1e821db35e68461bbf0d96dd7bd287f2 |
| Source note | uspto-grants-1993_02 |