HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentanone → HCID 59347806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentanone | HCID 8452 | — |
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | 1-(Dimethylamino)cyclopentanecarbonitrile | HCID 10773049 | — |
| Reactant | (2-Methoxyethyl)(methyl)amine hydrochloride | HCID 18670924 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 59347806 | HCID 59347806 | 82% |
Reaction Steps
The title compound (3.39 g; 82%) was prepared from N-(2-methoxyethyl)methylamine hydrochloride (2.84 g; 22.6 mmol), cyclopentanone (1.90 g, 22.6 mmol) and potassium cyanide (1.47 g; 22.6 mmol) in water (15 ml) in a similar manner to that described in D1. 1H NMR (CDCl3) δ: 1.83 (6H, m). 2.20 (2H, m), 2.48 (3H, s), 2.68 (2H, t), 3.46 (3H, s), 3.5 (2H, t).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07745642B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-e3b63cb316884a4c9f6038e4082ef5cd |
| Source note | uspto-grants-2010_06 |