HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 15052152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | HCID 14389216 | HCID 14389216 | — |
| Product | HCID 15052152 | HCID 15052152 | — |
Reaction Steps
In 10 ml of acetone was dissolved 1.27 g of quinuclidinol, and 1.86 g of methyl p-toluenesulfonate was added dropwise to the resulting solution. The mixture was stirred at room temperature, heated under reflux, and cooled to precipitate crystals. The crystals were collected by filtration and dried to give 2.81 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05183811 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-682031b6504f4c84b51150fe467c7648 |
| Source note | uspto-grants-1993_02 |