HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 19780040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 10445614 | HCID 10445614 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19780040 | HCID 19780040 | — |
Reaction Steps
Sodium borohydride (0.35 g, 0.0092 mol) was added at room temperature to 2-benzyloxy-5-acetyl-6-methylpyridin-3-carbonitrile (2.44 g, 0.0092 mol) in ethanol (60 mL). After 2 hours chloroform was added plus a few drops of acetic acid. After washing with water and brine, the chloroform solution was evaporated to give product which was not purified further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05185251 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-d281242594964377a93aa98f7623ae69 |
| Source note | uspto-grants-1993_02 |