HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 19780253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Methyl 6-(phenylmethyl)-2-pyridinecarboximidate | HCID 53840049 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19780253 | HCID 19780253 | — |
Reaction Steps
A mixture of methyl 6-benzyl-2-picoline imidate (0.81 g, 0.0036 moles) and ammonium chloride (0.21 g, 0.0039 moles) in ethanol (9 ml) was refluxed for 5 hours. The ethanol was removed in vacuo to give 6-benzyl-2-picoline amidine hydrochloride which was used in the final stage without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05185339 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-cbbe57ffb2994fe0adf991e5ff8a72d5 |
| Source note | uspto-grants-1993_02 |