HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 19780247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 53896835 | HCID 53896835 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19780247 | HCID 19780247 | — |
Reaction Steps
A mixture of methyl 6-(o-chlorobenzyl)-2-picoline imidate 5.5 g, 0.021 moles) and ammonium chloride (1.28 g, 0.024 moles) in ethanol (40 ml) was refluxed for 4 hours. The ethanol was removed in vacuo to give 6-(o-chlorobenzyl)-2-picoline amidine hydrochloride which was used in the final stage without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05185339 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-5fbed3513ee54e6bbff1079d2aed26cf |
| Source note | uspto-grants-1993_02 |