Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19096389 | HCID 19096389 | — |
Reaction Steps
A solution containing 1.1 g of pyridine-4-carboxaldehyde and 1.0 g of 2,4-pentanedione in 10 ml of N,N-dimethylformamide was saturated with hydrogen chloride gas at 20° C. The solution was stirred for 1 h at 20° C. and then for 2 h at 80° C. The solvent was evaporated in vacuo and the residue was crystallized from ethanol. Yield 0.17 g, mp 175°-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05185370 |
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| Source dataset | uspto-grants-1993_02 |
|---|
| ORD ID | ord-e5a9ef2d4b6244e5882d511e275f39f2 |
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| Source note | uspto-grants-1993_02 |
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