4-Cyanobenzaldehyde → HCID 19096392, compound

HRID 2081723Notes

Reaction equation

[C:1]([C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1)#[N:2].[CH3:11][CH2:12][C:13](=[O:19])[CH2:14][C:15](=[O:18])[CH2:16][CH3:17]>>[C:1]([C:3]1[CH:10]=[CH:9][C:6]([CH:7]=[C:14]([C:13](=[O:19])[CH2:12][CH3:11])[C:15](=[O:18])[CH2:16][CH3:17])=[CH:5][CH:4]=1)#[N:2]

Participants

Reactant 2

HCID 660424-Cyanobenzaldehyde

HCID 819233,5-Heptanedione

Product 1

HCID 19096392HCID 19096392, compound

Procedure

The produre described in Example 19 was repeated by using 2.6 g 4-cyanobenzaldehyde and 5.0 g 3,5-heptanedione. Yield 2.8 g, mp 59°-60° C.

Sources & evidence

ORD record: ord-be6d87371a394ed6af0ed554fbf8c5e7
Source dataset: uspto-grants-1993_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05185370

Reaction notes

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