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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2081951Generated: November 3, 2026

HCID 14858794, compound → HCID 14858793, compound

https://huagongshe.com/reaction/2081951

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 14858794HCID 14858794—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 14858793HCID 1485879386%

Reaction Steps

Compound VII (32 mg), obtained in Example 10, was dissolved in methanol (2 ml). Pd/C (10 mg) was added and the reaction mixture flushed with hydrogen and stirred for about 1.5 hours until all spotting material was gone, as determined by TLC in CH2Cl2 :ethylacetate (1:1), yielding 16.2 mg (86 percent yield) of Compound 5b.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05187086
Source datasetuspto-grants-1993_02
ORD IDord-2e4ffcfa218d421a9b022bb2bdb1eed0
Source noteuspto-grants-1993_02