HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14858794, compound → HCID 14858793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14858794 | HCID 14858794 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14858793 | HCID 14858793 | 86% |
Reaction Steps
Compound VII (32 mg), obtained in Example 10, was dissolved in methanol (2 ml). Pd/C (10 mg) was added and the reaction mixture flushed with hydrogen and stirred for about 1.5 hours until all spotting material was gone, as determined by TLC in CH2Cl2 :ethylacetate (1:1), yielding 16.2 mg (86 percent yield) of Compound 5b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187086 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-2e4ffcfa218d421a9b022bb2bdb1eed0 |
| Source note | uspto-grants-1993_02 |