HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 19779125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 19779127 | HCID 19779127 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19779125 | HCID 19779125 | — |
Reaction Steps
A mixture of 10 mL of formic acid and 25 uL of H2SO4 containing 0.25 the 5-nitro-2-(3-carbethoxypropyl)benzoisothiazol-3-one was heated in a 130° oil bath overnight. The reaction was cooled and then poured into 30 mL of water. After standing overnight, the mixture was filtered to yield 0.11 g of the title compound as a yellow solid, mp 183°-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187105 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-1e0b794edfd64597827f3e29c5ee37aa |
| Source note | uspto-grants-1993_02 |