Azido(trimethyl)stannane → HCID 178441898, compound

Participants

Reaction Steps

Reaction of 2-butyl-3-[(2'-cyanobiphenyl-4-yl)methyl]-5-methyl-3H-imidazo[1,2-b][1,2,4]triazole (from Steps B and C) with trimethyltin azide according to the procedure of Example 1, Step G, gave a 31% yield of the title compound as a light brown solid, mp 124°-125° C.; homogeneous by TLC in 90:10:0.1 CH2Cl2 -MeOH-AcOH.

Provenance & Evidence