HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanone, 1-bromo-1-phenyl- → HCID 178441924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanone, 1-bromo-1-phenyl- | HCID 90870 | — |
| Reactant | 3-amino-5-butyl-4-[(2'-cyanobiphenyl-4-yl)methyl]-4H-1,2,4-triazole | HCID 10065294 | — |
| Product | HCID 178441924 | HCID 178441924 | — |
Reaction Steps
Reaction of 3-amino-5-butyl-4-[(2'-cyanobiphenyl-4-yl)methyl]-4H-1,2,4-triazole (from Example 1, Step D) with 1-bromo-1-phenylacetone [A. C. B. Smith and W. Wilson, J. Chem. Soc., 1342 (1955)] according to the procedure of Example 1, Step E, gave an essentially quantitiative yield of the title compound as a yellow oil, suitable for use in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187179 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-198f837d02c84c8a9d8c82d7ceea0f0e |
| Source note | uspto-grants-1993_02 |