Azido(trimethyl)stannane → HCID 178441890, compound

Participants

Reaction Steps

Following the procedure of Example 1, Step G, 2-butyl-3-[(2'-cyanobiphenyl-4-yl)methyl]-5-methyl-6-phenyl-3H-imidazo[1,2-b][1,2,4]triazole (from Step B) was reacted with trimethyltin azide to give a 32% yield of the title compound as a brown solid, mp>108° C. (gradual); homogeneous by TLC in 90:10:0.1 CH2Cl2 -MeOH-AcOH.

Provenance & Evidence