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HRID2082067

反应详情

EQUATION

反应方程式

HRID 2082067 的结构方程式

REACTANTS

反应物

2
结构：[CH3][Sn]([CH3])([CH3])[N]=[N+]=[N-]
HCID5104973

Azidotrimethyltin(IV)

C3H9N3Sn

结构：CCCCc1nn2c(-c3ccccc3)cnc2n1Cc1ccc(-c2ccccc2C#N)cc1
HCID10410502

未命名化合物

PRODUCTS

生成物

1
结构：CCCCc1nn2c(-c3ccccc3)cnc2n1Cc1ccc(-c2ccccc2-c2nnn[nH]2)cc1
HCID178441891

未命名化合物

收率 46%

PROCEDURE

实验过程

Reaction of 2-butyl-3-[(2'-cyanobiphenyl-4-yl)methyl]-6-phenyl-3H-imidazo[1,2-b][1,2,4]triazole (from Step A) with trimethyltin azide according to the procedure of Example 1, Step G, gave a 46% yield of the title compound as a light brown solid, mp>70° C. (gradual): homogeneous by TLC in 90:10:0.1 CH2Cl2 -MeOH-AcOH.