HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azido(trimethyl)stannane → HCID 178441891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azido(trimethyl)stannane | HCID 5104973 | — |
| Reactant | 2-Butyl-3-[(2'-cyanobiphenyl-4-yl)methyl]-6-phenyl-3H-imidazo[1,2-b][1,2,4]triazole | HCID 10410502 | — |
| Product | HCID 178441891 | HCID 178441891 | 46% |
Reaction Steps
Reaction of 2-butyl-3-[(2'-cyanobiphenyl-4-yl)methyl]-6-phenyl-3H-imidazo[1,2-b][1,2,4]triazole (from Step A) with trimethyltin azide according to the procedure of Example 1, Step G, gave a 46% yield of the title compound as a light brown solid, mp>70° C. (gradual): homogeneous by TLC in 90:10:0.1 CH2Cl2 -MeOH-AcOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187179 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-dcc9a17852d84fecab66cf1f1ab3413a |
| Source note | uspto-grants-1993_02 |