HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 131717780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 15630270 | HCID 15630270 | — |
| Product | HCID 131717780 | HCID 131717780 | — |
Reaction Steps
A mixture of Boc-D-Trp-Phe-OBzl (1.0 g) and 24% methanolic ammonia (20 ml) was allowed to stand at room temperature in a sealed tube for 18 hours. After evaporation, the residual crystals were collected and recrystallized from a mixture of water and ethanol to give Boc-D-Trp-Phe-NH2 (0.63 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05187156 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-86577429f33441a29ea1b3acd16569dd |
| Source note | uspto-grants-1993_02 |