Potassium Carbonate → HCID 19778085, compound

Participants

Reaction Steps

In 10 ml of acetonitrile were stirred 2.7 g (10 mmol) of 1,3-dimethyl-4-(2,4-dichlorobenzyl)-5-hydroxypyrazole, 1.5 g (10 mmol) of 2,4-dichloropyrimidine and 1.5 g (11 mmol) of potassium carbonate with refluxing for 3 hours. After completing the reaction, the reaction mixture was purified as the same manner as described in Example 4 to give 1.63 g of 1,3-dimethyl-4-(2,4-dichlorobenzyl)-5-(2-chloropyrimidine-4-yloxy)pyrazole.

Provenance & Evidence