Diethyl Ether → HCID 13427304, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of phosphorus oxychloride ((1.53 g, 10 mmol) in anhydrous diethyl ether (20 ml), cooled at 0° C. under argon, is added a solution of 2.44 g (20 mmol) of phenethyl alcohol in diethyl ether (5 ml), followed by 2.02 g (20 mmol) of triethylamine in diethyl ether (5 ml). The mixture is stirred for 1 hour at 0° C., and then for 17 hours at room temperature. The final suspension is filtered, and the filtrate is evaporated to give 3.07 g of a colorless liquid.

Provenance & Evidence