HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 53651119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(4-Fluorobenzoyl)benzoic acid | HCID 82099 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53651119 | HCID 53651119 | — |
Reaction Steps
Thionyl chloride (1.6 ml) was added to a solution of 2-(4-fluorobenzoyl)benzoic acid (3.6 g) and pyridine (0.03 ml) in benzene (40 ml), followed by refluxing for an hour. The solvent was distilled off to give 2-(4-fluorobenzoyl) benzoyl chloride (IRνmaxNujol : 1790 cm-1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189043 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-433461696124480d9c4ea940407c06af |
| Source note | uspto-grants-1993_02 |