HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 2845263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-[4-(Methylamino)piperidin-1-yl]ethan-1-one | HCID 19761265 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 2845263 | HCID 2845263 | 65% |
Reaction Steps
A mixture containing 0.5 mol of the compound obtained in Stage A of Example 19, 0.5 M benzyl chloride and 1 M sodium carbonate in 650 ml of ethanol is refluxed for one night. The precipitate formed is filtered off, the solvent is evaporated, the evaporation residue is taken up in 1N hydrochloric acid and extracted with diethyl ether, and the ethereal extract is rendered basic with sodium hydroxide solution and extracted with ethyl acetate to obtain the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189045 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-dc67c0fc84074265b368bcbdce43d6ea |
| Source note | uspto-grants-1993_02 |