HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → N-[1-(ethoxycarbonylethyl)-piperid-4-yl]-N-methylpropionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | N-Methyl-N-(piperidin-4-yl)propionamide | HCID 19761222 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-[1-(ethoxycarbonylethyl)-piperid-4-yl]-N-methylpropionamide | HCID 19761283 | — |
Reaction Steps
7.4 g of the compound obtained in Stage C of Example 1 are dissolved in 10 ml of ethanol, then 4.73 ml of ethyl acrylate dissolved in 12 ml of ethanol are poured onto the solution. The mixture is left at room temperature for one night, and then concentrated in a rotary evaporator and distilled in a Kugelrohr to yield the compound in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189045 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-a719ef78986d43f6a1540eae9e37334b |
| Source note | uspto-grants-1993_02 |