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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2082373Generated: October 31, 2026

HCID 53946344, compound → HCID 14987373, compound

https://huagongshe.com/reaction/2082373

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53946344HCID 53946344—
CatalystPalladiumHCID 23938—
SolventBenzeneHCID 241—
ProductHCID 14987373HCID 14987373100.4%

Reaction Steps

A solution of (cis- and trans-) ethyl 5-(1-propenyl)-1-[2'-(1-triphenylmethyltetrazol-5-yl)biphenyl-4-yl-methyl]pyrrole-2-carboxylate (350 mg, 0.53 mmol) in benzene (35 ml) containing 5% Pd/C (35 mg) in a Paar bottle was placed on a Paar apparatus under 40 psi H2 and shaken for about 4 hours at room temperature. The mixture was suction filtered through Celite and concentrated to leave 350 mg of a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05189048
Source datasetuspto-grants-1993_02
ORD IDord-9e04f8091e484c7ba1c054056158e9f0
Source noteuspto-grants-1993_02