HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53946344, compound → HCID 14987373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53946344 | HCID 53946344 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 14987373 | HCID 14987373 | 100.4% |
Reaction Steps
A solution of (cis- and trans-) ethyl 5-(1-propenyl)-1-[2'-(1-triphenylmethyltetrazol-5-yl)biphenyl-4-yl-methyl]pyrrole-2-carboxylate (350 mg, 0.53 mmol) in benzene (35 ml) containing 5% Pd/C (35 mg) in a Paar bottle was placed on a Paar apparatus under 40 psi H2 and shaken for about 4 hours at room temperature. The mixture was suction filtered through Celite and concentrated to leave 350 mg of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189048 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-9e04f8091e484c7ba1c054056158e9f0 |
| Source note | uspto-grants-1993_02 |