HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2,6-Dichloro-4-(trifluoromethyl)phenyl]hydrazine → HCID 136341206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2,6-Dichloro-4-(trifluoromethyl)phenyl]hydrazine | HCID 688223 | — |
| Reactant | Propanedial, 2-oxo-, 1,3-dioxime | HCID 6399789 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 136341206 | HCID 136341206 | — |
Reaction Steps
A mixture of 2,6-dichloro-4-trifluoromethylphenylhydrazine (34 g), 2-oxopropanedial 1,3-dioxime (17 g) and ethanol (300 ml) was heated under reflux for 31/2 hours. The solvent was evaporated under reduced pressure and the residue triturated with light petroleum (bp 40°-60°) and filtered to give 2-oxopropanedial 2-(2,6-dichloro-4-trifluoromethylphenylhydrazone) 1,3-dioxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05189053 |
| Source dataset | uspto-grants-1993_02 |
| ORD ID | ord-3de0824770034b6b8b9bc5851d7b93a0 |
| Source note | uspto-grants-1993_02 |