HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-Chloro-4-ethoxy-6-dimethylamino-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2,4-Dichloro-6-(dimethylamino)-1,3,5-triazine | HCID 16985 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Dichlorotriazine | HCID 18348308 | — |
| Product | 2-Chloro-4-ethoxy-6-dimethylamino-1,3,5-triazine | HCID 23338142 | — |
Reaction Steps
A solution of sodium (0.46 g.) in ethanol (50 ml.) was added with stirring and waterbath cooling (25° C) to a solution of the dichlorotriazine (3.86 g.) from (a) in ethanol (50 ml.). Following the addition the solution was poured into ice water (250 ml.) and the product collected, dried and crystallised from petroleum as needles (2.5 g.) having a melting point of 124° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04082536 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-8330b79918314c6099f0d8671bbfa67d |
| Source note | uspto-grants-1978_04 |