HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70618533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 40592955 | HCID 40592955 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70618533 | HCID 70618533 | — |
Reaction Steps
To 0.44 g of benzyl t-butyloxycarbonyl-L-valyl-D-isoglutaminate (7, n = 2, X1 = L-valyl) at 22° C there is added 5 ml of a saturated solution of hydrogen chloride in ethyl acetate. After 20 minutes, 40 ml of ether is added and the precipitated salt is collected by centrifugation and carefully dried in vacuo to give benzyl L-valyl-D-isoglutaminate hydrochloride (10, n = 2, X1 = L-valyl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04082736 |
| Source dataset | uspto-grants-1978_04 |
| ORD ID | ord-f94eff23dba743da9f1113b730c914f8 |
| Source note | uspto-grants-1978_04 |